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008 170212s2015 gw | s |||| 0|eng d
020 _a9783319077499
_9978-3-319-07749-9
024 7 _a10.1007/978-3-319-07749-9
_2doi
035 _ato000557403
040 _aSpringer
_cSpringer
_dRU-ToGU
050 4 _aQD71-142
072 7 _aPNF
_2bicssc
072 7 _aSCI013010
_2bisacsh
082 0 4 _a543
_223
100 1 _aLu, Tian.
_eauthor.
_9463130
245 1 0 _aNanomaterials for Liquid Chromatography and Laser Desorption/Ionization Mass Spectrometry
_helectronic resource
_cby Tian Lu.
260 _aCham :
_bSpringer International Publishing :
_bImprint: Springer,
_c2015.
300 _aXVIII, 107 p. 97 illus., 16 illus. in color.
_bonline resource.
336 _atext
_btxt
_2rdacontent
337 _acomputer
_bc
_2rdamedia
338 _aonline resource
_bcr
_2rdacarrier
490 1 _aSpringer Theses, Recognizing Outstanding Ph.D. Research,
_x2190-5053
505 0 _aElectrospun Polyvinyl Alcohol Ultra-Thin Layer Chromatography of Amino Acids -- Homogeneous Carbon as Stationary Phase for Liquid Chromatography -- Preparation of Homogeneous Basal-Plane Carbon Nanorods and Its Application for Solid Phase Extraction -- Electrospun Nanofibers as Substrates for Surface-Assisted Laser Desorption/Ionization and Matrix-Enhanced Surface-Assisted Laser Desorption/Ionization Mass Spectrometry -- Synthesis of Fluorescent Carbon -- Future Work.
520 _aTian Lu's dissertation describes major advances in ultrathin-layer chromatography (UTLC), liquid chromatography and surface-assisted laser desorption ionization (SALDI), and matrix-enhanced SALDI (ME-SALDI) mass spectrometry. Lu describes the fabrication of electrospun polyvinyl alcohol (PVA) UTLC plates using an in-situ crosslinking electrospinning technique. The author improved the efficiency of PVA plates greatly compared to the efficiency of silica HPTLC plates.  Also highlighted in this thesis is an edge-plane based ordered-carbon surface that provides unique selectivity in liquid chromatography. Further developments include polar analytes, such as amino acids, nucleotides and nucleosides which can be well-retained and separated in the edge-plane ordered-carbon stationary phase. Also, the author studied and detected mass spectra of organic polymers as high as 900,000 Da, the highest molecular weight that has been studied by SALDI to date using the carbon nanofibrous substrate. This thesis has led to a number of publications in high-impact journals.
650 0 _achemistry.
_9161768
650 0 _aAnalytical Chemistry.
_9304189
650 0 _aPolymers.
_9303538
650 0 _aNanotechnology.
_9566290
650 1 4 _aChemistry.
_9161768
650 2 4 _aAnalytical Chemistry.
_9304189
650 2 4 _aNanotechnology.
_9566290
650 2 4 _aPolymer Sciences.
_9303539
710 2 _aSpringerLink (Online service)
_9143950
773 0 _tSpringer eBooks
830 0 _aSpringer Theses, Recognizing Outstanding Ph.D. Research,
_9567110
856 4 0 _uhttp://dx.doi.org/10.1007/978-3-319-07749-9
912 _aZDB-2-CMS
999 _c412496